Page 108
Notes:
conferenceseries
.com
Volume 8, Issue 2 (Suppl)
Chem Sci J 2017
ISSN: 2150-3494 CSJ, an open access journal
Euro Chemistry 2017
May 11-13, 2017
May 11-13, 2017 Barcelona, Spain
4
th
European Chemistry Congress
Structure characterization of 2,6-bis(2-hydroxyethyl)-1-phenylimidazo[1,5-c]-quinazoline-3,5-dione
A Szyszkowska
a
, I Zarzyka
a
, S Pawlędzio
b
, D Trzybińskib
and
K Woźniak
b
a
The Rzeszów University of Technology, Poland
b
University of Warsaw, Poland
T
he work presents the results of reaction product of 1-phenyl-2H,6H-imidazo[1,5-c]quinazoline-3,5-dione with 2 molar excess
ethylene oxide.
1-phenyl-2,6-bis(2-hydroxyethyl)imidazo[1,5-
c
]quinazoline-3,5-dione was isolated at high yield from the reaction mixtures and
identified based on the IR,
1
H-and
13
C-NMR spectroscopies. X-Ray diffractionmeasurement was also performed for the single-crystals
obtained by crystallization of crude product from ethanol. It was indicated that 1-phenyl-2,6-bis(2-hydroxyethyl)imidazo[1,5-c]
quinazoline-3,5-dione crystallizes in the monoclinic P2
1/n
space group with two molecules of compound in the asymmetric unit of
the crystal lattice. The crystal analysis revealed various types of molecular interactions in the crystal lattice of investigated compound.
To understand better the nature of packing of molecules in the crystal lattice of investigated compound the Hirshfeld surface analysis
was performed.
Biography
Agnieszka Szyszkowska graduated MA in 2014 at the University of Jan Kochanowski. She completed two courses of study: chemistry and biology. She started PhD
at the Rzeszów University of Technology in 2014.
szyszkowska.a@wp.plA Szyszkowska et al., Chem Sci J 2017, 8:2(Suppl)
http://dx.doi.org/10.4172/2150-3494-C1-009