Figure 2:
Reagents and conditions: (i) cyanamide, concentrated HCl, 1,4-dioxane, 80°C, 96%; (ii) POCl
3
, reflux, 7%; (iii) Piv
2
O, DMF, DMAP, Et
3
N, 60°C, 92%; (iv)POCl
3
, reflux, 75%.